• Media type: E-Article
  • Title: Nuclear magnetic resonance in the earth's magnetic field using a nitrogen-cooled superconducting quantum interference device
  • Contributor: Qiu, L. [Author]; Zhang, Y. [Author]; Krause, H.-J. [Author]; Braginski, A. I. [Author]; Burghoff, M. [Author]; Trahms, L. [Author]
  • Published: American Institute of Physics, 2007
  • Published in: Applied physics letters 91, 072505 (2007). doi:10.1063/1.2771060
  • Language: English
  • DOI: https://doi.org/10.1063/1.2771060
  • ISSN: 0003-6951
  • Keywords:
  • Origination:
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  • Description: The authors recorded nuclear magnetic resonance (NMR) spectra of water, benzene, fluorobenzene, and 2,2,2-trifluoroethanol in the earth's magnetic field (EMF) using a nitrogen-cooled superconducting quantum interference device (SQUID). In trifluoroethanol, the broadband detection characteristics of the SQUID with a noise floor of about 70 fT/root Hz enabled authors to simultaneously observe fluorine and proton spectra at 1940 and 2060 Hz Larmor frequency, reflecting their heteronuclear J coupling in the high-field limit without showing a measurable chemical shift. To reduce the noise in EMF-NMR, the authors suggest the use of frequency-adjusted averaging, which compensates line broadening due to EMF fluctuations. (C) 2007 American Institute of Physics.
  • Access State: Open Access