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Shabalin, A. G. [Author]; Zhang, M. [Author]; Yao, W. [Author]; Rysov, R. [Author]; Ren, Z. [Author]; Lapkin, D. [Author]; Kim, Y.-Y. [Author]; Assalauova, D. [Author]; Mukharamova, N. [Author]; Sprung, M. [Author]; Vartanyants, I. A. [Author]; Meng, Y. S. [Author]; Shpyrko, O. G. [Author]; 3University of California San DiegoDepartment of NanoEngineeringLa Jolla CA 92093-0448 USA [Author]; 2Deutsches Elektronen-Synchrotron DESYNotkestrasse 85 Hamburg 22607 Germany [Author]; 1University of California San DiegoDepartment of PhysicsLa Jolla CA 92093-0319 USA [Author]

Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging

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  • Media type: E-Article
  • Title: Mapping the 3D position of battery cathode particles in Bragg coherent diffractive imaging
  • Contributor: Shabalin, A. G. [Author]; Zhang, M. [Author]; Yao, W. [Author]; Rysov, R. [Author]; Ren, Z. [Author]; Lapkin, D. [Author]; Kim, Y.-Y. [Author]; Assalauova, D. [Author]; Mukharamova, N. [Author]; Sprung, M. [Author]; Vartanyants, I. A. [Author]; Meng, Y. S. [Author]; Shpyrko, O. G. [Author]; 3University of California San DiegoDepartment of NanoEngineeringLa Jolla CA 92093-0448 USA [Author]; 2Deutsches Elektronen-Synchrotron DESYNotkestrasse 85 Hamburg 22607 Germany [Author]; 1University of California San DiegoDepartment of PhysicsLa Jolla CA 92093-0319 USA [Author]
  • Published: International Union of Crystallography; 5 Abbey Square, Chester, Cheshire CH1 2HU, England, 2023-02-16
  • Language: English
  • DOI: https://doi.org/10.1107/S1600577523000814
  • Keywords: extra‐thick battery cathodes ; 3D mapping ; sphere of confusion ; Bragg coherent X‐ray diffractive imaging ; Bragg diffraction ; battery cathodes
  • Origination:
  • Footnote: Diese Datenquelle enthält auch Bestandsnachweise, die nicht zu einem Volltext führen.
  • Description: In Bragg coherent diffractive imaging, the precise location of the measured crystals in the interior of the sample is usually missing. Obtaining this information would help the study of the spatially dependent behavior of particles in the bulk of inhomogeneous samples, such as extra‐thick battery cathodes. This work presents an approach to determine the 3D position of particles by precisely aligning them at the instrument axis of rotation. In the test experiment reported here, with a 60 µm‐thick LiNi0.5Mn1.5O4 battery cathode, the particles were located with a precision of 20 µm in the out‐of‐plane direction, and the in‐plane coordinates were determined with a precision of 1 µm. ; A method to determine the 3D position of particles in Bragg coherent diffractive imaging experiments is proposed. Test measurements demonstrate depth‐resolution with a precision of 20 µm along the beam. image
  • Access State: Open Access