• Media type: E-Article
  • Title: Synthesis and Crystal Structure of Tris- [3,5-bis(trifluoromethyl)phenyl]arsine
  • Contributor: Dietzel, Pascal D. C.; Jansen, Martin
  • Published: Walter de Gruyter GmbH, 2004
  • Published in: Zeitschrift für Naturforschung B, 59 (2004) 3, Seite 345-347
  • Language: English
  • DOI: 10.1515/znb-2004-0320
  • ISSN: 1865-7117; 0932-0776
  • Keywords: General Chemistry
  • Origination:
  • Footnote:
  • Description: The title compound, As[C6H3(CF3)2]3, has been synthesised by Grignard reaction from arsenic trichloride and 3,5-bis(trifluoromethyl)phenylmagnesium bromide. It crystallises in the triclinic space group P1̅ with two formula units in the asymmetric unit. The most prominent feature of the crystal structure is the protrusion of a phenyl group of one molecule into the cavity at the base of the pyramid of a second molecule. The crystal structure is then built up by densely packing these units of interlocked molecules to form columns, which are arranged in parallel in a distorted hexagonal pattern
  • Access State: Open Access