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Medientyp: E-Artikel Titel: Analysis of highly polar compounds in groundwater samples from ammunition waste sites. Part I—Characterization of the pollutant spectrum Beteiligte: Preiss, Alfred; Elend, Manfred; Gerling, Susanne; Tränckner, Simone Erschienen: Wiley, 2005 Erschienen in: Magnetic Resonance in Chemistry Sprache: Englisch DOI: 10.1002/mrc.1609 ISSN: 0749-1581; 1097-458X Schlagwörter: General Materials Science ; General Chemistry Entstehung: Anmerkungen: Beschreibung: <jats:title>Abstract</jats:title><jats:p>Five groundwater samples from the former ammunition production site at Elsnig, Germany, were analyzed for highly polar components by LC–NMR and LC–MS. A variety of unknown pollutants could be identified. Possibilities and limitations of the combined use of LC–NMR and LC–MS techniques for on‐line identification are discussed. Further unknown components were identified through isolation by HPLC cuts and off‐line NMR and MS investigations. Most of the polar compounds in the investigated samples could also be quantified. Copyright © 2005 John Wiley & Sons, Ltd.</jats:p>