• Medientyp: E-Artikel
  • Titel: Microstructure and selected properties of the solution heat-treated MAR-M247 Ni-based superalloy fabricated via directional solidification
  • Beteiligte: Rakoczy, Łukasz; Grudzień-Rakoczy, Małgorzata; Cygan, Rafał; Kargul, Tomasz; Zielińska-Lipiec, Anna
  • Erschienen: Springer Science and Business Media LLC, 2024
  • Erschienen in: The International Journal of Advanced Manufacturing Technology
  • Sprache: Englisch
  • DOI: 10.1007/s00170-023-12785-0
  • ISSN: 0268-3768; 1433-3015
  • Schlagwörter: Industrial and Manufacturing Engineering ; Computer Science Applications ; Mechanical Engineering ; Software ; Control and Systems Engineering
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  • Beschreibung: <jats:title>Abstract</jats:title><jats:p>This work focuses on MAR-M247 Ni-based superalloy manufactured via directional solidification at various withdrawal rates (3.4 or 5.0 mm/min) and shell mold temperatures (1510 °C or 1566 °C) after solution heat-treatment (SHT). Observations and analyses of four casting variants were carried out using thermodynamic simulations, differential scanning calorimetry (DSC), X-ray diffraction (XRD), light microscopy (LM), scanning electron microscopy (SEM), X-ray spectroscopy (EDX), and tensile tests at ambient temperature. The solidus and liquidus temperatures were very similar for all variants and were in the range of 1263–1264 °C and 1356–1359 °C, respectively. The presence of the <jats:italic>γ</jats:italic>, <jats:italic>γ′</jats:italic>, MC carbides, and M<jats:sub>5</jats:sub>B<jats:sub>3</jats:sub> phases was confirmed. Microstructure differences were observed depending on the manufacturing parameters. The castings’ dendritic regions consisted of <jats:italic>γ′</jats:italic> precipitates surrounded by the matrix, with a mean size ranging from 0.203 to 0.250 μm, depending on the casting parameters. The amount of the MC carbides in the interdendritic spaces was in the range of 1.87–1.92%. The tensile tests determined that castings produced with preheat temperature of 1566 °C were characterized by higher elongation and slightly lower yield strength in comparison to 1510 °C.</jats:p>