• Medientyp: E-Artikel
  • Titel: Synthesis of Molybdenum Blue Dispersions Using Ascorbic Acid as Reducing Agent
  • Beteiligte: Gavrilova, Natalia; Myachina, Maria; Harlamova, Daria; Nazarov, Victor
  • Erschienen: MDPI AG, 2020
  • Erschienen in: Colloids and Interfaces
  • Sprache: Englisch
  • DOI: 10.3390/colloids4020024
  • ISSN: 2504-5377
  • Schlagwörter: Colloid and Surface Chemistry ; Chemistry (miscellaneous)
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  • Beschreibung: <jats:p>Stable molybdenum blue nanoparticles dispersions were synthesized using ammonium heptamolybdate and ascorbic acid. The effect of molar ratios of reducing agent/Mo and acid/Mo on the speed of formation and stability of the disperse system has been demonstrated. The particles were characterized by UV/vis, infrared (FTIR), nuclear magnetic resonance (NMR) spectroscopy, and dynamic light scattering (DLS) methods. The X-ray photoelectron spectroscopy (XPS) method confirmed the presence of reduced MoV in the structure of molybdenum oxide nanoclusters, the proportion of which was 30%.</jats:p>
  • Zugangsstatus: Freier Zugang