• Medientyp: E-Artikel
  • Titel: Xenon Plasma Focused Ion Beam Milling for Obtaining Soft X-ray Transparent Samples
  • Beteiligte: Mayr, Sina; Finizio, Simone; Reuteler, Joakim; Stutz, Stefan; Dubs, Carsten; Weigand, Markus; Hrabec, Aleš; Raabe, Jörg; Wintz, Sebastian
  • Erschienen: MDPI AG, 2021
  • Erschienen in: Crystals
  • Sprache: Englisch
  • DOI: 10.3390/cryst11050546
  • ISSN: 2073-4352
  • Schlagwörter: Inorganic Chemistry ; Condensed Matter Physics ; General Materials Science ; General Chemical Engineering
  • Entstehung:
  • Anmerkungen:
  • Beschreibung: <jats:p>We employ xenon (Xe) plasma focused ion beam (PFIB) milling to obtain soft X-ray transparent windows out of bulk samples. The use of a Xe PFIB allows for the milling of thin windows (several 100 nm thick) with areas of the order of 100 µm × 100 µm into bulk substrates. In addition, we present an approach to empirically determine the transmission level of such windows during fabrication by correlating their electron and soft X-ray transparencies. We perform scanning transmission X-ray microscopy (STXM) imaging on a sample obtained by Xe PFIB milling to demonstrate the conceptual feasibility of the technique. Our thinning approach provides a fast and simplified method for facilitating soft X-ray transmission measurements of epitaxial samples and it can be applied to a variety of different sample systems and substrates that are otherwise not accessible.</jats:p>
  • Zugangsstatus: Freier Zugang